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Structural basis of pharmacological chaperoning for human β-galactosidase.
[gm1 gangliosidosis]
GM
1
gangliosidosis
and
Morquio
B
disease
are
autosomal
recessive
diseases
caused
by
the
defect
in
the
lysosomal
β-galactosidase
(
β-
Gal
)
,
frequently
related
to
misfolding
and
subsequent
endoplasmic
reticulum-associated
degradation
.
Pharmacological
chaperone
(
PC
)
therapy
is
a
newly
developed
molecular
therapeutic
approach
by
using
small
molecule
ligands
of
the
mutant
enzyme
that
are
able
to
promote
the
correct
folding
and
prevent
endoplasmic
reticulum-associated
degradation
and
promote
trafficking
to
the
lysosome
.
In
this
report
,
we
describe
the
enzymological
properties
of
purified
recombinant
human
β-
Gal
(
WT
)
and
two
representative
mutations
in
GM
1
gangliosidosis
Japanese
patients
,
β-
Gal
(
R
201
C
)
and
β-
Gal
(
I
51
T
)
.
We
have
also
evaluated
the
PC
effect
of
two
competitive
inhibitors
of
β-
Gal
.
Moreover
,
we
provide
a
detailed
atomic
view
of
the
recognition
mechanism
of
these
compounds
in
comparison
with
two
structurally
related
analogues
.
All
compounds
bind
to
the
active
site
of
β-
Gal
with
the
sugar-mimicking
moiety
making
hydrogen
bonds
to
active
site
residues
.
Moreover
,
the
binding
affinity
,
the
enzyme
selectivity
,
and
the
PC
potential
are
strongly
affected
by
the
mono-
or
bicyclic
structure
of
the
core
as
well
as
the
orientation
,
nature
,
and
length
of
the
exocyclic
substituent
.
These
results
provide
understanding
on
the
mechanism
of
action
of
β-
Gal
selective
chaperoning
by
newly
developed
PC
compounds
.
Diseases
Validation
Diseases presenting
"detailed atomic view of the recognition mechanism of these compounds in comparison"
symptom
gm1 gangliosidosis
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